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Dearomatization of Indoles via a Phenol-Directed Vanadium- Catalyzed Asymmetric Epoxidation and Ring-Opening Cascade
An enantioselective dearomatization of indole derivatives was realized by the complexes derived from the vanadium complex VO(acac)2 and C2-symmetric bis-hydroxamic acid (BHA) ligands. The reaction proceeded via asymmetric epoxidation and ring-opening by the linked phenol cascade, affording 5a,6,10b,11-tetrahydrochromeno[2,3-b]indol-10b-ol derivatives in up to 83% yield and 98% ee under mild reaction conditions.
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Reference£º
Indole alkaloid derivatives as building blocks of natural products from?Bacillus thuringiensis?and?Bacillus velezensis?and their antibacterial and antifungal activity study,
Preparation of Indole Containing Building Blocks for the Regiospecific Construction of Indole Appended Pyrazoles and Pyrroles