In homogeneous catalysis, the catalyst is in the same phase as the reactant. The number of collisions between reactants and catalyst is at a maximum.In a patent, 252978-89-5, name is tert-Butyl 4-(1H-indol-4-yl)piperazine-1-carboxylate, introducing its new discovery. Recommanded Product: 252978-89-5
A method for preparing 2, 4, 6 – dicumylic (by machine translation)
A 2, 4, 6 – dicumylic preparation method, which relates to a 2, 4, 6 – dicumylic preparation method. The method of the invention is: nitrogen protection, under a certain temperature, the reaction of the phenol with a catalytic amount of the aluminum powder, aluminum powder completely disappeared after to, add a certain amount of ionic liquid is used as the cocatalyst, then adding alpha – methyl styrene, high performance liquid chromatography monitoring reaction, when the 2, 4, 6 – three dry bases phenol content when not continue to increase, adding dilute sulfuric acid to terminate the reaction, toluene extraction reaction product, atmospheric distillation to remove trace water in toluene, after cooling has white crystals, filtering to obtain the crude product; the crude product is then carried out for the 2nd toluene recrystallization to obtain content is more than 99% of the 2, 4, 6 – three dry bases phenol. This preparation method yield 64% the left and the right. Then the recrystallization mother liquor after removing the solvent, added with a certain amount of the phenol compound catalyst, continue to reaction, the mother liquor after the recovery, to the total amount is calculated, a yield of 95% or more. (by machine translation)
The proportionality constant is the rate constant for the particular unimolecular reaction. the reaction rate is directly proportional to the concentration of the reactant. I hope my blog about 252978-89-5 is helpful to your research. Recommanded Product: 252978-89-5
Reference£º
Indole alkaloid derivatives as building blocks of natural products from?Bacillus thuringiensis?and?Bacillus velezensis?and their antibacterial and antifungal activity study,
Preparation of Indole Containing Building Blocks for the Regiospecific Construction of Indole Appended Pyrazoles and Pyrroles