2532-74-3, 2-(1-Methyl-1H-indol-3-yl)ethanol is a indole-building-block compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
A mixture of 3.64 g 1-methyl-3-(2-hydroxyethyl)indole, 18 g methyltriphenoxyphosphonium iodide (J.O.C. 35 2323) and 75 ml dry N,N-dimethylformamide is stirred 2.5 hours at room temperature. Then 5 ml methanol are added, and the mixture is stirred 30 minutes. The mixture is poured into 500 ml dichloromethane and is washed successively with 50 ml portions of 5% aquous sodium thiosulfate, 10% NaOH, and water. The organic layer is dried briefly over magnesium sulfate and most of the solvent removed by evaporation, affording 1-methyl-3-(2-iodoethyl)indole., 2532-74-3
The synthetic route of 2532-74-3 has been constantly updated, and we look forward to future research findings.
Reference：
Patent; Syntex (U.S.A.) Inc.; US4255432; (1981); A;,
Indole alkaloid derivatives as building blocks of natural products from?Bacillus thuringiensis?and?Bacillus velezensis?and their antibacterial and antifungal activity study
Preparation of Indole Containing Building Blocks for the Regiospecific Construction of Indole Appended Pyrazoles and Pyrroles