914349-07-8,914349-07-8, tert-Butyl 3-(hydroxymethyl)-5-nitro-1H-indole-1-carboxylate is a indole-building-block compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Compound 4 (2.78 g, 9.5 mmol) was added to 40 ml of DCM, and then at 0 C., thionyl chloride (2.75 ml, 37.8 mmol) was added to the above reaction solution, and the reaction solution was moved to room temperature to react 1.5. h. The reaction mixture was quenched with water and extracted with DCM (X 3), dried over anhydrous magnesium sulfate, concentrated under reduced pressure, and separated on a silica gel column (PE: EA = 4:1) to give 2.0 g of a white solid. Yield 67%, purity 95.7%
As the paragraph descriping shows that 914349-07-8 is playing an increasingly important role.
Reference£º
Patent; Xihua University; Yang Lingling; Yan Jie; Su Huilin; Wang Zhouyu; Qian Shan; Wang Lijiao; (22 pag.)CN107915726; (2018); A;,
Indole alkaloid derivatives as building blocks of natural products from?Bacillus thuringiensis?and?Bacillus velezensis?and their antibacterial and antifungal activity study
Preparation of Indole Containing Building Blocks for the Regiospecific Construction of Indole Appended Pyrazoles and Pyrroles