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Green synthesis of predominant (1 1 1) facet CuO nanoparticles: Heterogeneous and recyclable catalyst for N-arylation of indoles
Well faceted CuO nanoparticles were synthesized by thermal-assisted green strategy at reflux temperature in a short period of time. A possible growth mechanism of such highly faceted nanostructures based on typical biomolecule-crystal interactions in aqueous solution is tentatively proposed. The large surface area (223.36 m2/g) and rich exposed active sites are expected to endow such nanostructures with excellent performances in catalysis as demonstrated here for remarkable catalytic activity with respect to the N-arylation of indoles. Nanoparticles were characterized by X-ray diffraction, scanning electron microscopy and transmission electron microscopy. Both the activity and selectivity of the N-arylation reactions could be tuned by varying the concentration of CuO nanoparticles. Nanoparticles catalyst were recycled and reused for further catalytic reactions with minimal loss in activity. A variety of indole derivatives afforded corresponding N-arylation product with excellent yields (up to 98%).
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Reference£º
Indole alkaloid derivatives as building blocks of natural products from?Bacillus thuringiensis?and?Bacillus velezensis?and their antibacterial and antifungal activity study,
Preparation of Indole Containing Building Blocks for the Regiospecific Construction of Indole Appended Pyrazoles and Pyrroles