In 2020.0 CHEM-EUR J published article about NITROGEN-CONTAINING BISPHOSPHONATES; PALLADIUM-CATALYZED PHOSPHONATION; PD(II)-CATALYZED PHOSPHORYLATION; REGIOSELECTIVE PHOSPHONATION; BIOLOGICAL EVALUATION; DIPHOSPHATE SYNTHASE; H-PHOSPHONATES; DRUG-DELIVERY; BONE; ALKYNES in [Cao Hao-Qiang; Liu Hao-Nan; Liu Zhe-Yuan; Qiao Bao-Kun; Zhang Fa-Guang; Ma Jun-An] Tianjin Univ, Tianjin Key Lab Mol Optoelect Sci, Dept Chem, Tianjin 300072, Peoples R China; [Cao Hao-Qiang; Liu Hao-Nan; Liu Zhe-Yuan; Qiao Bao-Kun; Zhang Fa-Guang; Ma Jun-An] Tianjin Univ, Tianjin Collaborat Innovat Ctr Chem Sci & Engn, Tianjin 300072, Peoples R China; [Zhang Fa-Guang; Ma Jun-An] Tianjin Univ, Joint Sch NUS & TJU, Int Campus, Fuzhou 350207, Peoples R China in 2020.0, Cited 120.0. The Name is 4′-Hydroxyacetophenone. Through research, I have a further understanding and discovery of 99-93-4. Safety of 4′-Hydroxyacetophenone
Herein we report a novel and straightforward protocol for the construction of valuable gem-BPs by means of proton-coupled electron-transfer (PCET)-triggered enamido C(sp(2))-H diphosphorylation. This reaction represents a rare example of realizing the challenging double C-P bond formation at a single carbon atom, thus providing facile access to a broad variety of structurally diverse bisphosphonates from simple enamides under silver-mediated conditions. Initial mechanistic studies demonstrated that the diphosphorylation involves two rounds of PCET-initiated radical relay process.
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Reference:
Indole alkaloid derivatives as building blocks of natural products from Bacillus thuringiensis and Bacillus velezensis and their antibacterial and antifungal activity study,
,Preparation of Indole Containing Building Blocks for the Regiospecific Construction of Indole Appended Pyrazoles and Pyrroles