Recently I am researching about SULFURYL FLUORIDE; BOND FORMATION; PHENOLS; ACIDS; ESTERS; SUFEX, Saw an article supported by the . Application In Synthesis of Mequinol. Published in WILEY-V C H VERLAG GMBH in WEINHEIM ,Authors: Zhang, GF; Wang, J; Guan, CF; Zhao, YY; Ding, CR. The CAS is 150-76-5. Through research, I have a further understanding and discovery of Mequinol
The synthesis of aryl phosphonates via nickel and palladium-catalyzed cross-coupling of aryl fluorosulfonates and phosphites is described. The products were obtained in good to excellent yields under mild conditions with broad functional group compatibility, employing either Pd(OAc)(2) and DPEPhos or the readily available NiCl2(dme) and Xantphos as catalytic systems. Noteworthily, the present C(sp(2))-P bond formation method could be applied to the direct conversion of phenols to the corresponding aryl phosphonates in one pot via reaction of phenols with SO2F2 and subsequent palladium-catalyzed cross-coupling.
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Reference:
Indole alkaloid derivatives as building blocks of natural products from Bacillus thuringiensis and Bacillus velezensis and their antibacterial and antifungal activity study,
,Preparation of Indole Containing Building Blocks for the Regiospecific Construction of Indole Appended Pyrazoles and Pyrroles